A Novel 2‐D Structure Constructed from Copper Complexes and Bi‐Capped Tungsten‐Based Keggin Clusters.

Ya-Bing Liu,Li-Wei Fu,Wei-Jie Duan,Li-Na Xiao,Yang-Yang Hu,De-Chuan Zhao,Hai-Yang Guo,Xiao-Bing Cui,Ji-Qing Xu

ChemInform（2014）

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摘要

The novel polyoxometalate [Cu(en)2(H2O)]{[Cu0.5(en)]3 [VVWVI6.5WV3V IV4.5O42Cu(en) 2]}·3.5H2O is hydrothermally synthesized from a mixture of Na2WO4, V2O5, CuSO4, (COOH)2 (molar ratio of 2:1:1:2), en, and H2O (autoclave, pH 7, 180 °C, 3 d, 60% yield).

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